Tailored synthesis in nanoparticle permanent magnets (NPPMs)

Top: Differential scanning calorimetry (DSC) of metal eutectic for Fe16N2, demonstrating low-temperature melting.
Differential scanning calorimetry (DSC) of metal eutectic for Fe16N2, demonstrating low-temperature melting.

CMI researchers from Ames National Laboratory conducted the activity for this highlight

Innovation 
Identified and prepared promising rare earth-free, non-critical metal eutectics to serve as low-temperature sintering aids and grain-boundary phases for Fe16N2 and Sm2Fe17N3

Achievement
Suitable non-magnetic metal eutectics with melting points below the NPPMs’ decomposition temperatures, but higher than projected operating temperatures, have been prepared for Fe16N2 and Sm2Fe17N3

Significance and Impact

  • An appropriate eutectic compound will enable a scalable process that allows for uniform densification of the NPPMs with superior density to bonded magnets for high saturation magnetization while optimizing the grain boundaries to achieve near theoretical coercivity.
  • Next step is to investigate reactivity and wettability of metal eutectics with magnetic phases and impact to magnetic properties as powders.

Hub Target Addressed 
Accelerated magnet discovery and maturation.

DSC of metal eutectic for Sm2Fe17N3
DSC of metal eutectic for Sm2Fe17N3