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Indirect detection of infinite-speed MAS solid-state NMR spectra

TitleIndirect detection of infinite-speed MAS solid-state NMR spectra
Publication TypeJournal Article
Year of Publication2017
AuthorsPerras, FA, Venkatesh, A, Hanrahan, MP, Goh, TW, Huang, WK, Rossini, AJ, Pruski, M
JournalJournal of Magnetic Resonance
Volume276
Pagination95-102
Date Published03
Type of ArticleArticle
ISBN Number1090-7807
Accession NumberWOS:000395851800013
Keywordsadiabatic pulses, c-13 nmr, chemical-shift, D-HMQC, Magic-angle-turning, manipulation, metal-organic frameworks, Metal-organic-framework, Molecular Biology, natural-abundance, nuclear-magnetic-resonance, physics, Platinum NMR, sensitivity enhancement, side-band, Spectroscopy, spin-1/2 nuclei, ultra-fast mas
Abstract

spectra of heavy spin-1/2 nuclides. For these nuclides, the combination of fast MAS and 1H detection provides a high sensitivity, which rivals the DNP-enhanced ultra-wideline SSNMR. The new pulse sequences were used to determine the Pt coordination environments in a complex mixture of decomposition products of transplatin and in a metal-organic framework with Pt ions coordinated to the linker ligands. (C) 2017 Elsevier Inc. All rights reserved.

DOI10.1016/j.jmr.2017.01.010
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3D Catalysis

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Royalty

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LDRD

Alternate JournalJ. Magn. Reson.