%0 Journal Article
%J Journal of Magnetic Resonance
%D 2007
%T HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids
%A Amoureux, J. P.
%A Trebosc, J.
%A Wiench, J.
%A Pruski, M.
%K 3-DIMENSIONAL LATTICE CONNECTIVITIES
%K CORRELATI
%K HMQC
%K j-coupling
%K J-COUPLINGS
%K MAS
%K MAS NMR
%K MQMAS
%K NATURAL-ABUNDANCE SAMPLES
%K polarization
%K QUADRUPOLAR NUCLEI
%K R-INEPT
%K solid-state nmr
%K STATE NMR EXPERIMENTS
%K STMAS
%K THROUGH-BOND CONNECTIVITIES
%K TRANSFER
%M ISI:000243568900001
%P 1-14
%R 10.1016/j.jmr.2006.09.009
%V 184
%X Hetero-nuclear coherence transfers in HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids are analyzed. 1D and 2D schemes are considered under MAS for the general case of multi-spin systems SIn, (n <= 4), where S is an observed nucleus. These results are also discussed in the context of high-resolution schemes featuring MQMAS or STMAS. The theoretical predictions are verified experimentally in a series of 1D and 2D experiments performed at 9.4 and 18.8 T. (c) 2006 Elsevier Inc. All rights reserved.
%8 Jan
%9 Article
%@ 1090-7807